Tool: Macro X-ray fluorescence scanner
Organization
National Research Council, Institute of Heritage Science - XRAYLab
Last checked date
17-12-2024
Description
The mobile Macro-XRF scanner (MXRF) consists of a spectrometric head equipped with a low power microfocus X-ray tube (30W) with a Rh anode coupled to a focusing polycapillary optic. The spot of the beam coming out from the primary X-ray source is about 55 microns at 10 keV at a focus distance of 14.7 mm. The detection system is positioned in a 90-degree geometry with respect to the beam direction. It consists of 6 SDD detectors (with 50mm2 active area collimated to 40mm² for a total active area of 240mm² and <130 eV energy resolution at 5.9 keV each) operated in parallel. This experimental set-up improves drastically the chemical sensitivity and the detection limits of the device. A single scan with the XY axes travel system installed on the MAXRF instrument can cover an area of 110x90cm2. The system operates with a continuos scanning with a maximum speed up to 150 mm/sec. in A Z axis coupled to laser triangulation device is used for a dynamic correction spectrometric head position in order to maintain the source-sample distance uniform during the scanning. Due to the high intensity of the primary X-ray beam and the large solid angle covered by the multi-detectors system, measurements are usually made with a dwell-time per pixel in the range of 10ms. The entire scanning area (about 1m2) is mapped in about 3 hours by operating the scanning with a lateral resolution of 1mm and a scanning speed of 100mm/sec. The lateral resolution of the elemental images is in the range of 250-1000 microns depending on the artworks dimensions. The system is equipped with a central unit (CU) for controlling the operational parameters of the scanner and to operate a dynamic analysis (full deconvolution of the pixel spectra on the fly) providing real-time elemental distribution images to users. The Macro-XRF scanner can be configured to perform scans in both vertical and horizontal geometries.
Output and data types
Image/RGB
Image/Gray scale
Dataset/2D
Dataset/Data package (images, spectra, other)
Report
metadata (experimental conditions, comments relative to the point)
data interpretation
Impact on object or sample
Noncontact (no physical contact)
Nondestructive (no permanent damage or alteration)
Noninvasive (no physical alteration)
Manufacturer
XRAYlab (ISPC-CNR)
Acquisition areas
110x90cm2 (XY- Vertical scanning)
110x20cm2 (XZ - Horizontal scanning)
Working distances
Close-range (0.01 - 0.1 m)