Description
The plasma laboratory contains six instruments: two MC-ICPMS, a quadrupole ICP-MS, and a ICP-OES
The optical ICP (inductively coupled plasma) is a modern compact, bench top Thermo iCAP Pro, with a verticalradial plasma view. This instrument will be used for major- and trace-element analysis of liquid samples (water, dissolved geological, archaeological, environmental, or forensic material). This instrument can also be connected to one of the laser-ablation instruments for major-element analysis of ablated solid materials. Limits of quantification are typically in the range of 0.05 to 10 ppb, depending on the element.
The ICP-MS instrument (Thermo iCAP-TQ) is an versatile instrument that can be used to analyze trace-elements in both solutions and solid material (laser-ablation). It contains two mass analysers on either side of a collision-reaction cell to separate masses from each other, resulting in interference free masses and therefore accurate measurements. In addition, it has a collision cell to remove interferences. In a collision cell gasses such as He, O2, and H are used to selectively collide of react with certain ions derived from the plasma or the sample matrix, separating the interference and target ions. Routinely, we analyse >40 elements from Li to U quasi-simultaneously in several minutes per sample. Samples are mainly introduced as solution via a quartz cyclonic spray chamber. The iCAP-TQ can also be attached to a femto-second or nano-second laser (see below) to analyse trace-elements in solid materials. Limits of quantification for liquid samples are generally, depending on the element, between 0.1 ppt and 0.1 ppb
The new standard Thermo Neoma MC-ICP-MS is equipped with 11 Faraday cups, which can be connected to eleven standard 1011 Ω and four 1013 Ω amplifiers. In addition, it is equipped with one electron multiplier. High resolution (mass resolving power up to ~12000) allows for resolving molecular isobaric interferences (e.g., 40Ar16O+ on 56Fe+). Samples are introduced as solution via a quartz dual cyclonic spray chamber (‘wet plasma’) or an Aridus III or Apex Omega desolvator (‘dry plasma’). In addition, the nano- and femto-second lasers can ablate solid metals and silicates and introduce them as aerosols to the plasma. We routinely analyse radiogenic isotopes (Rb/Sr, Sm/Nd,, Lu/Hf Pb, U/Th) as well as non-traditional stable isotopes (Li, Si, Fe, Cu, Zn, Sr, Ba).
Acquisition areas
teeth
water samples
glass
materials
bones
forensic human materials
metals
cultural heritage (paint, wood, glaze, etc.)
rock